Professor Joseph M. Fox
212 Lammot Du Pont Laboratory
302-831-0191
jmfox@udel.edu
Lectures are held in Wolf 100, Mondays 3:35–5:35 pm
Office hours: Mondays 11-12, or by appointment. Contact me by email to schedule an appointment
Lectures are captured via UD Capture, which may serve as a resource. However, note that the blackboard is used in class (which is not captured on the video)
http://udcapture.udel.edu/2013f/chem333-010/
Laboratory
The director of the organic teaching laboratories is Dr. Geoffrey Sametz, sametz@UDel.Edu
QUESTIONS ABOUT THE LABORATORY SHOULD BE DIRECTED TO DR. SAMETZ
The laboratory syllabus can be found here:
https://sakai.udel.edu/portal/site/4d966bd4-c04b-4b73-97fd-df1989cdb2fc
All info is under the "resources" folder; including the lab schedule, grading/notebook format.
For a tutorial on using reaxys:
Teaching Assistant
The teaching assistant for Chem 333 is Danielle Shacklady McAtee. Her office hours will be held in room 208 LDL at the following times:
Tuesday 12.30-1.30 pm; Thursday 11.30-12.30 pm
Textbooks:
For students taking both lab and lecture (Chem 333-010): Chem 331/333 LAB MANUAL
For students taking only the lecture (Chem 333-011): Organic Spectroscopic Structure Determination, author = Douglass Taber
Restated:
If you are in section Chem 333-010 (lab + lecture), then the required books are as follows:
• 331/333 LAB MANUAL (new or used OK)
• You do NOT need to purchase Organic Spectroscopic Structure Determination
If you are in Chem 333-011 (lecture only), then the required books are
as follows:
• Organic Spectroscopic Structure Determination (new or used OK)
-
•You do NOT need to purchase the 331/333 LAB MANUAL
Note- chapters 12-14 from the lab manual will be handed out in class, and are posted BCT Ch 11_14c.pdf
Clickers
Either generation of clickers (gen 1 or 2) will work for this class.
Grading and Exams
Grading for the lecture part of this course will be determined based on the average (50% each) of a midterm and final exam.
Midterm will be in class on 10/21
Final will be during finals week
Exam 1
exam 1 333_2013 answer key_ A.pdf
exam 1 333_2013 answer key_ B.pdf
OLD EXAMS AND PROBLEMS
333Exam12009.pdf 2009_Exam1_answers.pdf
333Exam2_2009 Chem333Exam2_2009_answers
Ch14added problems answers to end of chapter 14 problems.pdf
IR problem set 2013.pdf IR problem set 2013 answers.pdf
UV_combinedProblems.pdf UV_PS answers.pdf
2001 final exam.pdf 2001 final exam answers.pdf
old exam 2 questions.pdf Old Exam 2 answers.pdf
postMidtermReview.pdf (answers are provided as links)
final exam review questions.pdf final exam review_answers.pdf
final exam review UV answers.pdf
KEY HANDOUTS (additional handouts linked in each lecture below)
1H and 13C NMR essentials part 2.pdf
Lecture schedule
Lecture 1 (9/9): Introduction to Structure Determination by Spectroscopy; IHD and 13C NMR spectroscopy.
READ: Chapter 12 in Lab manual or Chapter 1 in Organic Spectroscopic Structure Determination
HANDOUT: Lecture1.pdf, Carbon NMR essentials.pdf
PROBLEMS: Complete end of chapter 12 problems 1–10 from Lab Manual
Answers (Answers to problems 1-10 were covered in class)
Lecture 2 (9/16): Problem Solving with 13C NMR spectroscopy
REQUIRED VIEWING: Lecture 2 is posted online. Please watch the following in sequential order
https://www.youtube.com/watch?v=SWozhUpRf4o
https://www.youtube.com/watch?v=JCfoP8anSr0
https://www.youtube.com/watch?v=vsC367BxbFM
https://www.youtube.com/watch?v=1H9hatQ5_Mg
http://www.youtube.com/watch?v=HRbv1HL0AuI&feature=youtu.be
PROBLEMS: Complete end of chapter 12 problems 11–20 from Lab Manual
Answers
video answers for problems 1-12
https://www.youtube.com/watch?v=YtgPb11LRRM
https://www.youtube.com/watch?v=ncUcbbH3UUw
https://www.youtube.com/watch?v=1RZlxIEXm_A
https://www.youtube.com/watch?v=weC5MWWpDNA
Lecture 3 (9/23): 1H NMR spectroscopy
READ: Chapter 13 in Lab Manual or Chapter 2 in Organic Spectroscopic Structure Determination
HANDOUT: 1H NMR lecture guide , 1H NMR tables
PROBLEMS: Complete end of chapter 13 problems 1–10 from Lab Manual
Lecture 4 (9/30): Read Chapter 14 in Lab Manual or Chapter 2 in Organic Spectroscopic Structure Determination Problem Solving with 1H NMR spectroscopy
PROBLEMS: Complete end of chapter 14 problems 1–5 from Lab Manual
HANDOUT: Structure solving guide
Lecture 5 (10/7): Problem Solving with 1H NMR spectroscopy
PROBLEMS: Complete end of chapter 14 problems 6–10 from Lab Manual
Lecture 6 (10/14): more Problem Solving with 1H NMR spectroscopy, midterm review
MIDTERM EXAM (10/21)
also refer back to Dr. Koh's website for old midterms
Lecture 7 (10/28): IR spectroscopy
HANDOUT: 1) IR lecture A, case studies 2) IR lecture B , 3) handout: combined tables for NMR, UV, IR and MS
PROBLEMS: IR problemset (answers combined with UV problems)
Lecture 8 (11/4): Mass spectrometry
HANDOUT: MS lecture notes
Lecture 9 (11/11): MS, in class problem solving
HANDOUT: 1) UV-vis Lecture notes
HOMEWORK: problem set and answers
Required viewing: UV-vis lecture:
http://www.youtube.com/playlist?list=PLTDTR0hbdr_OtPRBu8arB6NOXcjoOZo76
Lecture 10 (11/18): UV-vis, in class problem solving
Lecture 11 (11/25): Problem solving with multiple techniques
Review questions for the final
Final Exam (12/5): Final exam review