Copyright " 2000 Douglass F. Taber

 

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CHAPTER 26: FRIEDEL-CRAFTS ALKYLATION AND ACYLATION

Data Report Sheet


A. Preparation of BHT

<><><><><><><>
Molecular weight<><>Grams<><>Moles<><>

p-Cresol:

t-Butyl alcohol:

Limiting reagent is:

Theoretical yield of BHT

mol:

g:

Actual yield of BHT

g:

Percent yield:

Melting point:



B. Preparation of para-Di-t-butylbenzene


<><><><><>Molecular weight<><>Grams<><>Moles

t-Butylbenzene:

 

t-Butyl chloride:

Limiting reagent is

Theoretical yield of p-di-t-butylbenzene

mol:

g:


Actual yield of p-di-t-butylbenzene

g:

Percent yield:

Melting point:

C. Friedel-Crafts synthesis of an unsymmetrical diaryl ketone

<><><><><>Molecular weight<><>Grams<><>Moles

Xylene:

Oxalyl chloride:

AlCl3:

Anisole:

Theoretical yield of ketone

mol:

g:


Actual yield of ketone

g:

Percent yield:

Melting point:



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