Copyright Ó 2000 Douglass F. Taber

Data Report Sheet

1. Preparation of Cyclohexanone:
   
   Equation:
   
   
   Grams cyclohexanol used:
   
   Moles cyclohexanol used:
   
   Moles cyclohexanone expected:
   
   Grams cyclohexanone recovered:
   
   Moles cyclohexanone recovered:
   
   Percentage yield:
   
   Boiling point range:
   
   B. Preparation of Adipic Acid:
   
   Equation:
   
   
   Milligrams cyclohexanone used:
   
   Millimoles cyclohexanone used:
   
   Millimoles adipic acid expected:
   
   Milligrams adipic acid recovered:
   
   Millimoles adipic acid recovered:
   
   Percent yield:
   
   Melting point range:
   
   C. Oxidation of p-Nitrobenzyl Alcohol:
   
   Equation:
   
   
   Grams p-nitrobenzyl alcohol used:
   
   Millimoles p-nitrobenzyl alcohol used:
   
   Millimoles p-nitrobenzaldehyde expected:
   
   Grams p-nitrobenzaldehyde recovered:
   
   Millimoles p-nitrobenzaldehyde recovered:
   
   Percent yield:
   
   Melting point range:
   
   D. Haloform Reaction:
   
   Equation:
   
   
   Milligrams acetophenone used:
   
   Millimoles acetophenone used:
   
   Millimoles benzoic acid expected:
   
   Milligrams benzoic acid recovered:
   
   Millimoles benzoic acid recovered:
   
   Percent yield:
   
   Melting point range:
   
   E. Reduction of Benzophenone:
   
   Equation:
   
   
   Milligrams benzophenone used:
   
   Millimoles benzophenone used:
   
   Millimoles diphenylmethanol expected:
   
   Milligrams diphenylmethanol recovered:
   
   Millimoles diphenylmethanol recovered:
   
   Percent yield:
   
   Melting point range:
   
   Attach Infrared spectrum:
   
   F. Reduction of p-Nitrobenzaldehyde:
   
   Equation:
   
   
   R_f value for p-nitrobenzaldehyde:
   
   R_f value for p-nitrobenzyl alcohol:
   
   Time for complete reaction (disappearance of p-nitrobenzaldehyde):
   
   Comments: