Copyright " 2000 Douglass F. Taber
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CHAPTER 26: FRIEDEL-CRAFTS ALKYLATION AND ACYLATION
Data Report Sheet
A. Preparation of BHT
<><><><><><><>Molecular weight<><>Grams<><>Moles<><>
p-Cresol:
t-Butyl alcohol:
Limiting reagent is:
Theoretical yield of BHT
mol:
g:
Actual yield of BHT
g:
Percent yield:
Melting point:
B. Preparation of para-Di-t-butylbenzene
<><><><><>Molecular weight<><>Grams<><>Moles
t-Butylbenzene:
t-Butyl chloride:
Limiting reagent is
Theoretical yield of p-di-t-butylbenzene
mol:
g:
Actual yield of p-di-t-butylbenzene
g:
Percent yield:
Melting point:
C. Friedel-Crafts synthesis of an unsymmetrical diaryl ketone
<><><><><>Molecular weight<><>Grams<><>Moles
Xylene:
Oxalyl chloride:
AlCl3:
Anisole:
Theoretical yield of ketone
mol:
g:
Actual yield of ketone
g:
Percent yield:
Melting point:
Comments: